The facility's X-ray instrumentation is built around a Rigaku MicroMax 003 X-ray generator.
X-Ray Source
X-Ray Source
Crystal Diffraction
Our system is fitted with a Saturn 944 HG CCD for detecting crystal diffraction. The goniometer is equipped with a Micro-glide 3-axis head that allows automated centering. Crystals can be mounted manually, but the facility also has an ACTOR robot that can mount crystals from up to 5 ALS or Uni pucks. With this system, up to 80 crystals can be automatically screened in a single run. The robot can then collect the best samples on a single puck for a synchrotron trip, or devise and execute a strategy for in-house data collection.
Methods Library
Crystallization and Condition Screening
Calero G, Cohen AE, Luft JR, Newman J, and Snell EH. "Identifying, studying and making good use of macromolecular crystals". Acta Cryst. F 2014 (F70): p 993-1008. DOI: 10.1107/S2053230X14016574
Collecting Diffraction Data
Mueller M, Wang M, and Schulze-Briese C. "Optimal fine φ-slicing for single-photon-counting pixel detectors". Acta Cryst. D 2012 (D68): p 42-56. DOI: 10.1107/S0907444911049833
Krojer T, Pike ACW, and von Delft F. "Squeezing the most from every crystal: the fine details of data collection." Acta Cryst. D 2013 (D69): p 1303-13. DOI: 10.1107/S0907444913013280